Preparation and Study of the Structural, Thermal and Spectral Properties of lead Titanate

Abstract

Compound with the chemical formula (PbTiO3) were prepared using solid-state reaction method. The compound were calcined at 1000 oC for 4 hr. The structural properties of X-ray diffraction were studied and the results showed that the samples are tetragonal perovskite structure, the particle size was homogeneous of the samples, and increase the apparent density on the actual density. The results of the atomic force microscope (AFM) analysis showed a grain size, roughness and root mean square. TGADSC analysis shows low weight loss. The results of the infrared spectra for sample showed that the constant force of the bond (k) increased as a result of the stretching vibration Ti-O bond.